A new type of degradable synthetic polymer was prepared by Rh-catalyzed three-component polymerization of a bis(diazocarbonyl) compound, bis(1,3-diketone), and tetrahydrofuran. The resulting polymer was highly sensitive to mild acidic conditions and degraded into a combination of well-defined low molecular weight compounds. With this unique degradability, the polymer could be utilized as an environmentally friendly polymeric material.
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